Quantitative Chromatographic Analysis gives the procedure for measuring fentanyl in whole blood at the subnanogram level using mass- and nitrogen-sensitive spectrometry!

Quantitative Chromatographic Analysis provides practical guidance concerning all critical factors involved in successful quantitative chromatographic analysis, details the fundamental principles of gas, high-performance liquid, and thin-layer chromatographic instrumentation, and reveals how these considerations affect quantitative assays.

Quantitative Chromatographic Analysis documents the significance of response index, data processing, internal and external standards, injector systems, solvent focusing, temperature programming, pumping systems, and extracolumn dispersion!

Offering practical examples to demonstrate the diversity of samples capable of being analyzed, Quantitative Chromatographic Analysis:

• describes derivatization techniques
• examines liquid, solid, and supercritical fluid extractions
• considers solid phase microextraction for extraction and concentration
• explains cryofocusing for improved resolution
• highlights the use of chiral columns for enantiomeric separation
• summarizes preconcentrating with chelating columns
• discusses membrane diffusion for sample extraction
• and more!

Outlining analysis from sample collection and preparation to processing data and reporting results, Quantitative Chromatographic Analysis is an outstanding reference for chromatographers; analytical, physical, pharmaceutical, oil, petroleum, clinical, forensic, environmental, and synthetic chemists, biochemists, and biotechnologists; and upper-level undergraduate and graduate students in these disciplines.

Contents

Introduction to Quantitative Chromatographic Analysis

1. The Critical Factors that Govern a Successful Quantitative Chromatographic Analysis
2. Sample Collection, Transport, and Storage
3. Sample Preparation
4. The Chromatography Detector
5. Processing Chromatographic Data

Quantitative Gas Chromatographic Analysis

6. Gas Chromatographic Apparatus for Quantitative Analysis
7. Gas Chromatography Applications

Quantitative Liquid Chromatography Analysis

8. Liquid Chromatographic Apparatus for Quantitative Analysis
9. Liquid Chromatography Applications

Thin-Layer Chromatography

10. Thin-Layer Chromatography Apparatus
11. Thin-Layer Chromatography Applications

Index

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