A Practical Guide
edited by
Sue Ann Scheppers Wercinski
This comprehensive, up-to-the-minute reference contains extensive descriptions of proven sampling methods for chemical analyses. The book focuses on the myriad applications of solid phase microextraction (SPME) for laboratories analyzing dirty sample matrices and requiring high sample throughput, quick sample turnaround time, and low detection levels.
Provides a sound theoretical basis for SPME, plus highly detailed descriptions of pharmaceutical, environmental, food science, forensic, and toxicological applications!
Written by the researchers who developed the technique and industry scientists
who have used and improved it in practice, Solid Phase Microextraction:
- discusses the full range of SPME methods for laboratories performing routine analyses
- compares SPME performance with traditional sample preparation methods such as headspace, purge and trap, liquidliquid extraction, Sohxlet extraction, and direct injection
- defines practical techniques for chromatographers who want to develop their own SPME methods
- describes commercially available fibers and classes of compounds used in SPME analysis
- addresses EPA, FDA, and other government regulatory agency standards
- explains SPME's proven performance from samples with the lowest possible analyte concentration and highest possible levels of contamination
- and more!
Featuring an extensive index and emphasizing problem solving for busy professionals, this accessible, user-friendly resource is essential reading for analytical, organic, medicinal, and food chemists; chromatographers; toxicologists; forensic scientists; laboratory managers and technicians; and upper-level undergraduate and graduate students in these disciplines.
Contents
Solid Phase Microextraction Theory
Sue Ann Scheppers Wercinski and Janusz Pawliszyn
Method Development with Solid Phase Microextraction
Zelda Penton
SPME Fibers and Selection for Specific Applications
Robert E. Shirey
Pharmaceutical Applications
Stephen Scypinski and Ann-Marie Smith
Environmental Applications
Brian MacGillivray
Food and Flavor Applications
Xiaogen Yang and Terry L. Peppard
Forensic and Toxicology Applications
José R. Almirall and Kenneth G. Furton
New Developments in SPME
Ralf Eisert and Janusz Pawliszyn
Appendix